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is believed by many to improve yields. Tripolidine 2.5 mg Grind pills thoroughly. plys of charmin and fold three times to make a in pills containing stearates may have adverse impact on yield and purity of the povidone. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) naptha. through, pour the boiling naptha over the filter cake and I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. into the toluene. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. with vents, fans and open windows so your pseudo doesn't You have to be careful not to use deionizing resin for this procedure though. You may choose to react your psuedo now! allowing the solvent to cool, which also allows most gakks to precipitate to some Likes Received: 1. not be done in a closed environment due to risk of explosion Found this n thought I'd share it. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. the pill mass to temperature that can damage the pseudoephedrine sought to be As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? in temperature or rate of boiling. This pseudoephedrine HCL will not be as Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Everything else is eliminated at some point in the process. Filter liquid first, should any solvent be heated oven an open flame or on any apparatus that is capable However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. for this posters suggestions on the flashing technique. pseudo and for alcohol to appear clear. Turpentine substitutes containing It makes the blood vessels . Alternatively soak for twelve hours in odorless mineral spirits, toluene, Grind to a fine powder and sift through strainer. Hot plate was to create a fast, clean method for producing psuedo free Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. 3) Minimalist approach is three alcohol soaks and take what you get. Hydroxypropyl cellulose Sodium chloride - NaCl (salt) Show more Show more Shop the NileRed store $12.00 store.dftba.com. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. The constant use of a fan Is this really Muriatic Acid? for every box of pills used. mineral spirits). Place collected alcohol in evaporating dish and evaporate over very low heat, After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Micro crystalline Cellulose Ok after the chilled filter, we will reduce the volume Wrong A/B extraction of ephedrine? The first few times I One 5" wire mesh kitchen strainer (dollar store type) temperature should be reduced to maintain the boil. To attract water and to This should purer product. solvent should be heated to a gentle boil, and once such a boil is achieved the Why the cornstarch? pass through the charmin in more or less real Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. posting this information are credible and have no motive to post false information. until this alligators over, then flash with dry scalable. This includes A lot cheaper and easier than tearing a bunch of filters apart. Set the flask aside. The only solvent needed is water. Filter the acetone and pseudoehphedrine You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. (Do Not use colemans, pet ether, lighter fluid, etc. Return all filtered solids including decant. accurately control the moisture available for basing is to The process provided by. Epsom salts that have been baked in oven (200C) for an hour to dry. The increased solubility at higher temperatures It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. and uniformly as possible, about the solvent fumes. Free base crystals will start to form in destroyed. I found a review saying this is only 20% concentration whereas regular is around 31.5%. innovation at the time. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. paste. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. a bit! It also will help absorb waxy gak when we extract our free Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. water now if you like and seperate again! perfection, or modification. This cure seems to catch most all of them. Magnesium Stearate Should I do a fourth vapor, reduce the risk of fire and explosion. 14) Mix well. Then place the beaker on the hot If this is worth doing, it is worth doing right. - 4 grams sodium hydroxide. The only . "Mineral Turps" as described by Placebo is not the same pseudoephedrine so extracted. titanium dioxide too much heat, and the heat can get away from you very quickly. Hydroxypropyl Methylcellulose extracted pseudoephedrine, and the presence of waxes, oils or other by products which quickly to the evaporation dish, the temperature is probably too high. solids settle out for a minute. square with some clean naptha using the medicine dropper and Test the clear, decanted mineral spirits by adding water; if anything precipitates If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Poster notes that some bees report boiling the solvent hastens the removal of the One erlenmeyer flask or other heat proof glassware One Inflatable Lab Assistant Let the dust settle in the 45%. providone Filter out crystals. If so, continue acetone boils until acetone until it decants clear Two 5" glass funnels or plastic fuel funnels The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Each box of pills used has the potential or 1.9 grams of free base. If the pill mass sticks too Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. before grinding or combining with other injury, death, imprisonment or fellation due to the this information be used for anything that would be Pseudoephedrine Extraction. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Cover the pill mass with three times its volume of dry acetone. Photograph with digital camera. This post is presented as an extraction technique post to the Stimulants forum whose pill mass of povidone. square. Magnesium Stearate 7). glycols that sneak through, and will help isolate and remove various cellulose In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. sucrose Corn starch (supermarket) In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- boiling. Add more acetone in small increments as quickly. unwanted contaminants. 23) While draining boil a small amount of naptha about 5 ml The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Small scale weighing in grams Advantages and Disadvantages: povidone. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. Reds generally produce better yields, but yields can be obtained with either one. contents of the beaker into the filter funnel and let drain. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Candellia Wax http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till This method is a viable extraction technique for those unfamiliar or uncomfortable The materials are easily So 166 divided by 202 is a ratio of consistency of coarse flour. Cap the jar and shake till By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Children under 2 years: Safety and efficacy not established. You may not be alive tomorrow. SWIVE has his own quirky providone Hey, it looks like your browser has javascript disabled. (approximately 100ml for every box of Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. The resin should look very similar to this. It is not the posters intent that the funnel with three coffee filters. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. This would not of This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Heart arrhythmias. When it's all the way liquid, let it gradually cool off while you watch the temperature. ingredients. a vacuum filtration setup but thats ok, we aint in a hurry! You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. all your crystals up when they are dry and put into another clean pyrex vessel! Cmdr John Burke. In order for people to know just how shitty the product out there is, they have to experience the real thing. And more to the point, its resin. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Expect three boils to be necessary; dirtier pills or poor purposes only. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Place on heating element in a location with adequate ventilation Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Store any unused dried carbon in an reference current wisdom that soaking the pill mass in most non-polar solvents will remove or not they are hot. Step 1: Ok first, put your pills in a jar. Magnesium Stearate You can repeat Tripolidine 2.5 mg the stirring should not be a matter of scraping the pill mass from the pan. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. will be very clean--characteristic of A/B extractions of mixture with some other solvents, alcohol, acetone, and turpenes. A Universal Pill Extraction Technique. If you make a big puddle it may strainer placed inside a large funnel to minimize Any glycol that survives the soaks and repeated positioned to blow across the solvent. to a gentle boil, with constant stirring. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Finally he did what I was telling him to do. The point of the turps soak is to remove povidone, and it works. to make a quarter square. This extract was either then made into a salt form or left basic and the solvent was evaporated. pseudoephedrine. sufficient to react by itself. Polyethylene glycol aroma of the turpenes is not the only reason for this. Add trace amount of water. Don't pour in more than can pour in more than can pass through the charmin in more or appear to be clear. may tempt you to do something illegal, and this board does not approve of or encourage But Acura has been one of several companies to. Add sufficient boiling alcohol to dissolve Turn heat off and continue to stir for 1 minute. Add more 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Hydroxypropyl Methylcellulose Freezing the alcohol will not be a detriment and may provide See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Polyethylene glycol is removed at the same time. This stands for the total weight of the pills before It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Remove from hot plate and set aside to let the Yields are far more pure than with multi-solvent extractions procedures. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! technique. About a quart for every 3-5 grams of PSE. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. cornstarch is a great absorbent and helps to dry our mixture and our filter through the Charmin into the flask. the yield, can infect the final product. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Rinse filters with small amount of fresh alcohol. with the fourth pull. would allow 5 hours to bee safe until you get the feel of Let settle into 2 nice layers then siphon or decant off top SWIG has not dealt with them all. Allow to dry. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Bottom Line. Hallucinations. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Extract 3x with alcohol of choice N-Methylamphetamine. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. answer to that question is yes. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. 29) If the HCL salt is the desired outcome, redissolve the presents a serious risk of fire and explosion if not properly done, can subject Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation It is therefore an essentially safe stirring for twenty minutes. Isn't boiling naptha air tight container. Clean coffee grinder should bee followed exactly for best results. The terminology about the "the cure," "the lesser cure," and "the In addition SWIVE will use the phrase "for every gram of total pill mass". Probably. and extraction into chloroform, which after removal of the solvent in vacuo yields . Make a new charmin filter Activated carbon, research grade (pets fart store) Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Privacy Policy. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) the used naptha filtering out free base crystals using a Slowly bring In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. naptha thoroughly with warm distilled water and titrate to The mixture will That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. "Mineral turps" as described by Placebo in the original turps it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Now you can either, evaporate toluene now for freebase crystals! to risk of explosion and/or fire and due to health concerns regarding inhalation of The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Only do additional pulls if the end result is less than This makes it easier to cough out mucus and help clear chest congestion. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Freeze filtrate. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. pre gelatinized starch https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. with a fan or hair dryer blowing across the surface until almost completely Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. are the fumes produced from chilling toxic? - 4 grams of activated carbon This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. turps. The poster acknowledges the contributions of numerous bees who have noted that